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Methods of isolation and identification of natural compounds

ВКБ.9.03

Вибіркова дисципліна для ОП

First

2022/2023

6 Semester

4

Р03. Skill to describe chemical data in symbolic form. Р08. To know principles and procedures of physical, chemical, physicochemical research methods, typical equipment, and instruments. Р09. Skill to plan and perform a chemical experiment, to apply suitable methods and techniques for preparation of solutions and reagents. Р11. Skill to describe properties of aliphatic, aromatic, heterocyclic, and organometallic compounds... Р12. To know main synthesis pathways in organic chemistry, including f interconversion of functional group and formation of carbon-carbon, carbon-heteroatom bonds. Р14. Skill to perform experimental work to test hypotheses and investigation of chemical phenomena and regularities. Р17. Ability to work individually or in a group, to obtain results within a limited time with an emphasis on professional honesty and scientific integrity. Р20. Skill to interpret the experimental data and to correlate this data with corresponding theories in chemistry.

Full-time form

1. Know the program material of the basic course of organic chemistry at the bachelor's level. 2. Have basic knowledge of stereochemistry and mechanisms of organic reactions at the bachelor's program level. 3. Possess basic skills of laboratory techniques and basics of organic synthesis at the bachelor's program level.

Types of chromatography (horizontal, flow, two-dimensional, radial and others), chromatography on fixed and unfixed sorbent layer, basic laws and techniques of experimental chromatography on columns on alumina and silica gel, the possibility of separation and quantification of natural compounds by chromatography on paper.

1. Minaeva V.O. Chromatographic analysis. – Cherkasy "CNU B. Khmelnitsky", 2013. – 284 p. 2. Rax V.A., Yesaulenko A.M. Modern chromatography on the ridge waves of progress. – Kyiv: Avanpost, 2014. – 168 p. 3. Kulikov A.Y. Thin-layer chromatography: theoretical foundations and practical use. – Kharkiv: V.N. Karazin Kharkiv National University, 2011. – 260 p. 4. Lastukhin Yu.O. Chemistry of natural organic compounds. – Lviv "Intelect-Zakhid", 2004. – 560 p. 5. Kovalev V.M., Pavliy O.I., Isakova T.I. Pharmacognosy with the basics of plant biochemistry. – Kharkiv: Prapor. – 2000. – 704 p. 6. Bioorganic Chemistry / Y.I. Gubsky [et al.]; ed. prof. I.V. Nezhenkovska. – Vinnytsia: New Book, 2021. – 647 p.

Сombination of lectures and work in the laboratory

Semester control includes laboratory works, tests and surveys on the topics of tests. Evaluation is carried out on a 100-point system. The maximum / minimum number of points that can be obtained by a student during the semester assessment is 100 points / 60 points.

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