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Capillary gas chromatography and capillary electrophoresіs

ВБ.6.07

Вибіркова дисципліна для ОП

Second

2023/2024

3 Semester

3

Apply the acquired knowledge and understanding to solve new qualitative and quantitative problems of chemistry. Be able to clearly and unambiguously convey the results of one's own research to a professional audience and/or non-specialists. Collect, evaluate, and analyze the data needed to solve complex chemistry problems using appropriate data processing methods and tools. Plan and organize experimental research in chemistry using modern equipment, competently process research results and draw reasonable conclusions. Interpret experimentally obtained data and correlate them with relevant theories in chemistry.

Full-time form

Possession of knowledge of basic courses of analytical, general, inorganic, organic and physical chemistry. Basic knowledge of separation and sample preparation methods, basics of chromatographic analysis, electrochemistry, mathematical statistics and analytical materials science. Possession of skills of work in laboratory of analytical chemistry. Ability to statistically process the results, work with modern computers and various sources of information.

In-depth theoretical and practical study of gas chromatography methods. Types of capillary columns and directions of their application. The main approaches to optimization of methods of gas chromatographic analysis of objects of different nature. Theoretical basis of separation methods based on the phenomenon of electrophoresis. Varieties of methods and analytical capabilities of each of them. Advantages and new possibilities of separation of complex mixtures in open capillaries. Hardware of the method. Methods of obtaining and processing primary data, calculation of the content of components of complex mixtures. The most important sources of information about the use of capillaries in gas chromatography and electrophoresis.

1. Lysenko O.M., Kovalchuk T.V., Zaitsev V.M. Basics of gas chromatography. Part 1. K.: Kyiv VOC, 2014. 2. Lysenko O.M., Kovalchuk T.V., Zaitsev V.M. Basics of gas chromatography. Part 2. K.: Kyiv VOC, 2014. 3. Lysenko O.M., Kovalchuk T.V., Levchyk V.M., Zaitsev V.M. Workshop on gas chromatography. K.: Kyiv VOC, 2013. 4. Heiger D. High performance capillary electrophoresis – Germany 03|00, Publication Number 5968-9963E. 5. Lysenko O.M., Nabyvanets B.Y. Introduction to chromatographic analysis. K.: "Corvin Press". 2005. - P. 38-53. 6. David W. Grant. Capillary Gas Chromatography (Part of SSS). 2009. 7. Harvey D. Modern analytical chemistry – The McGraw-Hill company, US, 2000.

Lectures, laboratory work

Semester control includes work in practical classes, including oral examinations, tests and surveys on the topics of tests. Evaluation is carried out on a 100-point system. The maximum / minimum number of points that can be obtained by a student during the semester assessment is 100 points / 60 points.

Ukrainian