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Features of the synthesis of new complex oxide and coordination compounds

ВБ.3.08

Вибіркова дисципліна для ОП

Second

2023/2024

3 Semester

3

P02. Deeply understand the main facts, concepts, principles, theories related to the subject area mastered during the master's program, use them to solve complex tasks and problems, as well as conduct research in the relevant field of chemistry. P03. Apply the acquired knowledge and understanding to solve new qualitative and quantitative problems of chemistry. P9. Collect, evaluate and analyze the data needed to solve complex chemistry problems using appropriate methods and data tools P09. Collect, evaluate, and analyze the data needed to solve complex chemistry problems using appropriate data processing methods and tools. P14. Interpret experimentally obtained data and correlate them with relevant theories in chemistry.

Full-time form

1. Know general, inorganic, physical chemistry, crystal chemistry, coordination chemistry, solid state chemistry, the basics of inorganic materials science, physicochemical and physical methods of researching chemical compounds. 2. To have the basics of synthetic chemistry, using modern approaches, to plan synthesis; choose the necessary reaction conditions and synthesis medium; methods of studying matter and its properties.

"Features of the synthesis of complex oxide and coordination compounds" is one of the special chemical educational disciplines, the subject of which forms professional ideas about the strategy, planning, techniques and technical means of synthesis of complex oxide and coordination compounds, understanding the peculiarities of synthesis at high and low temperatures, hydrothermal synthesis, synthesis in non-aqueous solvents, synthesis in melts and in solution-melts, mechanochemical synthesis, sol-gel method, electrosynthesis. The study of the chemistry of complex compounds consists of: - a course of lectures reflecting fundamental theoretical issues, modern achievements and prospects for the development of science; - a laboratory workshop covering the use of physico-chemical methods of analysis to study the composition, structure and properties of complex oxides and complex compounds, and a scientific experiment that develops skills, scientific thinking, that details theoretical information; - independent work, which involves studying and deepening knowledge of the main sections of synthetic chemistry of inorganic and complex compounds with the use of additional literature

1. V.V. Skopenko, V.Ya. Zub, Coordination chemistry. Practicum K.: Kyiv University Publishing House. 2002. 2. Direct synthesis of coordination and organometallic compounds/Edited by A.D.Garnovskii and B.I.Kharisov/ Elsevier, 1999, 244 p. 3. J.A.Davies, Ch.M.Hockensmith, V.Yu.Kukushkin, Yu.N.Kukushkin. Synthetic coordination chemistry: principles and practice. World Scientific Publishing Co.Pte. Ltd., 2009, 390 p 4. Rao C. N. R., Goopalakrishnan J. New Direction in Solid State Chemistry. London: 199 5. Direct synthesis of coordination compounds / Ed. V.V. Ckopenko. Kyiv: Venturi, 1997.

Lectures (using computer presentations), laboratory work, independent work

- semester assessment: The maximum/minimum number of points that can be obtained by a student: 60 points /36 points, namely: 1. Modular control paper 1 with topics 1-4: РН1.1– 10 points / 6 points. 2. Modular control paper 2 with topics 6-14: РН1.2, РН1.3 – 20 points /10 points. 4. Abstract / computer presentation 1: RN 1.1 RN 1.2 – 15 points / 10 points. 5. Abstract / computer presentation 2: RN 1.3, RN 2.1:– 15 points / 10 points. - final evaluation (in the form of a written exam). The maximum/minimum number of points that can be obtained by a student: 40 points /24 points. Learning outcomes that will be evaluated: PH 1.1, PH 1.2, PH 1.3, PH 1.4, PH 2.1, PH 2.2. Form of conduct: written work. Types of tasks: one theoretical question for 10 points, 15 test questions for 30 points. To receive an overall positive grade in the discipline, the grade for the exam cannot be less than 24 points.

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