Infopaket

Scientific and industrial practice

ОК.11

Обов’язкова дисципліна для ОП

Second

2023/2024

3 Semester

6

• independently plan and conduct experimental research; • carry out the synthesis of initial and final substances, as well as possess the skills of conducting a physical and chemical experiment to obtain the substances provided for in the plan course (or master's) work; • separate the reaction mixture and purify the interaction products (extraction, simple and fractional distillation at atmospheric pressure and in a vacuum, distillation with steam, recrystallization, fractional crystallization, thin-layer and column chromatography); • calculate concentrations, weights of substances, prepare solutions; • select the conditions for the synthesis of organic, inorganic and polymer compounds; • interpret EPR NMR spectra, X-rays, diffractograms, 14-, FP-, and UV spectra in the visible region, DTA and TG curves, chromatograms, voltammograms, etc.; • perform elemental analysis of organic substances; • discuss experimental results; • draw conclusions and generalizations.

• rules of safety and behavior in the chemical laboratory, safe techniques work and conducting research; • modern methods of searching for scientific information; • basic methods and techniques of preparation and conducting physical and chemical research.

Topics, individual tasks and calendar plans for the master's course of scientific and industrial practice are formed taking into account the directions of scientific research work of the department's teachers, approved course and master's topics works, already completed and protected coursework, as well as completion of students who during the period of study engaged in scientific work in scientific circles, etc. To enable students to choose a research topic and for the purpose of formation the future intern is responsible for the results of practice at the department, in advance they form a list of topics that correspond to the main scientific directions of the department, including current ones.

1. Clayden, J.; Greeves, N. and Warren, S. (2012) Organic Chemistry. Oxford University Press. pp. 1–15. ISBN 0-19-927029-5. 2. Elschenbroich, C. (2006) Organometallics 3rd Ed., Wiley-VCH 3. Morrison, Robert T.; Boyd, Robert N. and Boyd, Robert K. (1992) Organic Chemistry, 6th ed., Benjamin Cummings. ISBN 978-0136436690. 4. Greenwood, Norman N.; Earnshaw, Alan (1997). Chemistry of the Elements (2nd ed.). Butterworth-Heinemann. ISBN 978-0-08-037941-8. 5. Henry Marshall Leicester; Herbert S. Klickstein (1951). A Source Book in Chemistry, 1400-1900. Harvard University Press. p. 309. 6. Kiefer, D. M. (1993). "Organic Chemicals' Mauve Beginning". Chem. Eng. News. 71 (32): 22–23. doi:10.1021/cen-v071n032.p022. 7. Streitwieser, Andrew; Heathcock, Clayton H.; Kosower, Edward M. (2017). Introduction to Organic Chemistry. New Delhipages=3–4: Medtech (Scientific International, reprint of revised 4th edition, Macmillan, 1998). ISBN 978-93-85998-89-8.

practice

Attending practice and completing tasks - 0-50 Performance of an individual task - 0-10 Drawing up a report on practice - 0-15 Practice defense - 0-25 The sum of points required for crediting practice results 51-100

Ukrainian