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Modern methods of organic microimpurities identification

ВКБ.3.08

Вибіркова дисципліна для ОП

Second

2021/2022

8 Semester

2

Р01. Knowledge to understand key chemical concepts, essential facts, concepts, principles, and theories relating to natural sciences, life and earth sciences, as well as chemical technologies at a level sufficient for professional application and to enable further deep understanding of specialized fields of chemistry. Р04. Knowledge to understand basic patterns and types of chemical reactions as well as their characteristics. Р08. To know principles and procedures of physical, chemical, physicochemical research methods, typical equipment, and instruments. Р16. Skill to perform computer calculations related to chemical problems by using standard and special software, abilities to analyse and display results.

Full-time form

Basic knowledge of BSc cources of General chemistry, Physics, Math, Inorganic Chemistry, Physical Chemistry, Organic Chemistry, Chemical and Instrumental Methods of Quantitative Analysis and "Physical methods of analysis in chemistry".

Methods of detection and identification of organic compounds in environemental samples, biological probesand technological mixtures are studied. These methods are based on mass-spectrometric (MS) analysis in conjunction with preliminary separation gas chromatography, liquid chromatography and capilary electrophoresis. The approaches and practical aspects of above methods application for wide range of analytical tasks in the fields of ecological monitoring, forensics, doping analysis, biochemical studies and authentication of products are concidered.

1. A. Lebedev, Comprehensive Environmental Mass Spectrometry, ILM Publications, 2012. 2. R. M. Silverstein, F. X. Webster, D.J. Kiemle, D. L. Bryce, Spectrometric Identification of Organic Compounds, 8th Edition, Wiley 2014. 3. J. H. Gross, Mass Spectrometry. A Textbook. 3rd Edition. Springer, 2017. 4. R. K. Boyd, C. Basic, R. A. Bethem, Trace Quantitative Analysis by Mass Spectrometry, John Wiley & Sons, 2008.

Lectures

The evaluation is based on a 100-point system. Semester control includes control works and home practical works. The maximum / minimum number of points that can be obtained by a student during the semester assessment is 60 points / 36 points. The final assessment is conducted in the form of an exam. The maximum / minimum number of points that can be obtained by a student on the exam is 40 points / 24 points.

Ukrainian