Methods of determining organic components and elemental composition of substances

Course: Chemistry (Bachelor)

Structural unit: Faculty of Chemistry

Title
Methods of determining organic components and elemental composition of substances
Code
ВКБ.3.08
Module type
Вибіркова дисципліна для ОП
Educational cycle
First
Year of study when the component is delivered
2022/2023
Semester/trimester when the component is delivered
8 Semester
Number of ECTS credits allocated
3
Learning outcomes
P06 Understand the periodic law and the periodic system of elements, describe, explain and predict the properties of chemical elements and compounds based on them. P07 Apply the basic principles of quantum mechanics to describe the structure of atoms, molecules, and chemical bonds. P15 Ability to use acquired knowledge and skills for calculations, display and modeling of chemical systems and processes, processing experimental data. P18 Demonstrate knowledge and understanding of basic facts, concepts, principles and theories in chemistry. P21 Monitor and analyze scientific sources of information and professional literature.
Form of study
Prerequisites and co-requisites
Know the basics of inorganic, organic and physical chemistry, chemical and instrumental methods of quantitative analysis and the course "physical research methods in chemistry". Successful completion of basic courses in general chemistry, physics and mathematics at the undergraduate level.
Course content
As part of the course "Mass spectrometry and X-ray fluorescence in analysis", the physicochemical basics of the mass spectrometry (MS) method and its combination with previous methods of separation: gas and liquid chromatography are studied. Tandem mass spectrometry, laser desorption-ionization mass spectrometry, isotope ratio mass spectrometry, and inductively coupled plasma mass spectrometry approaches are also studied. The basics of X-ray fluorescence spectral analysis (XFRS), formation of an analytical signal, methods of qualitative and quantitative analysis are also studied. Peculiarities and practical nuances of the application of these methods are considered for solving a wide range of chemical and analytical problems: analysis of environmental objects, biomedical research and control of modern technological processes, etc.
Recommended or required reading and other learning resources/tools
1. O.V. Ishchenko, S.V. Gaidai, O.A. Byeda, Mass spectrometry., K.: Kyiv University. 2018. – 244 p. 2. A. Lebedev, Comprehensive Environmental Mass Spectrometry, ILM Publications, 2012. 3. J. H. Gross, Mass Spectrometry. A Textbook. 3rd Edition. Springer, 2017. 4. R. K. Boyd, C. Basic, R. A. Bethem, Trace Quantitative Analysis by Mass Spectrometry, John Wiley & Sons, 2008 5. K.M. Belikov, O.I. Yurchenko X-ray fluorescence analysis, Study guide, Kharkiv, 2012, 52 p. 6. R.M. Silverstein, F.X. Webster, D.J. Kiemle, D. L. Bryce, Spectrometric Identification of Organic Compounds, 8th Edition, Wiley 2014. 7. J. T. Watson, O. D. Sparkman, Introduction to mass spectrometry, Wiley 2007. 8. J. Greaves, J. Roboz, Mass Spectrometry for the Novice, Taylor & Francis, 2014.
Planned learning activities and teaching methods
Сombination of lectures and practical exercises
Assessment methods and criteria
Semester control includes homework and tests. The evaluation is based on a 100-point scale. The maximum / minimum number of points that can be obtained by a student during the semester assessment is 60 points / 36 points. The final assessment is conducted in the form of an exam. The maximum / minimum number of points that can be obtained by a student in the exam is 40 points / 24 points.
Language of instruction
Ukrainian

Lecturers

This discipline is taught by the following teachers

Sergei Aleksandrovich Alekseev
Analytical Chemistry Department
Faculty of Chemistry
Serhii Oleksandrovych Leliushok
Analytical Chemistry Department
Faculty of Chemistry

Departments

The following departments are involved in teaching the above discipline

Analytical Chemistry Department
Faculty of Chemistry
Analytical Chemistry Department
Faculty of Chemistry