Infopaket

Mass spectrometry and X-ray fluorescence in analysis

ВБК.1.08

Вибіркова дисципліна для ОП

First

2022/2023

8 Semester

3

P06. Understand the periodic law and the periodic table of elements, describe, explain and predict the properties of chemical elements and compounds based on them. P07. Apply the basic principles of quantum mechanics to describe the structure of atoms, molecules, and chemical bonds. P15. The ability to use the acquired knowledge and skills for calculations, display and modeling of chemical systems and processes, as well as processing experimental data. P18 Demonstrate knowledge and understanding of basic facts, concepts, principles and theories in chemistry. P21 Monitor and analyze scientific sources of information and professional literature.

Know the basics inorganic, organic and physical chemistry; chemical and instrumental methods quantitative analysis; course "Physical research methods in chemistry". Successful mastery basic courses in general chemistry, physics and mathematics at the undergraduate level.

As part of the course "Mass spectrometry and X-ray fluorescence in analysis", the physicochemical basics of the mass spectrometry (MS) method and its combination with previous separation methods: gas and liquid chromatography are studied. Tandem mass spectrometry, laser desorption-ionization mass spectrometry, isotope ratio mass spectrometry, and inductively coupled plasma mass spectrometry approaches are also studied. The basics of X-ray fluorescence spectral analysis (XFRS) are studied, in particular, the principles of generating an analytical signal and methods of qualitative and quantitative analysis by this method. Peculiarities and practical nuances of using the specified methods for solving a wide range of chemical and analytical problems: analysis of environmental objects, biomedical research and control of modern technological processes, etc.

1. О. В. Іщенко, С.В. Гайдай, О.А. Бєда, Мас‐спектрометрія., К.: ВПЦ "Київський університет". 2018. – 244 с. 2. A. Lebedev, Comprehensive Environmental Mass Spectrometry, ILM Publications, 2012. 3. J. H. Gross, Mass Spectrometry. A Textbook. 3rd Edition. Springer, 2017. 4. R. K. Boyd, C. Basic, R. A. Bethem, Trace Quantitative Analysis by Mass Spectrometry, John Wiley & Sons, 2008 5. К.М. Бєліков, О.І. Юрченко Рентгенофлуоресцентний аналіз: Навчальний посібник, Харків, 2012, 52 с. 6. R. M. Silverstein, F. X. Webster, D.J. Kiemle, D. L. Bryce, Spectrometric Identification of Organic Compounds, 8th Edition, Wiley 2014. 7. J. T. Watson, O. D. Sparkman, Introduction to mass spectrometry, Wiley 2007. 8. J. Greaves, J. Roboz, Mass Spectrometry for the Novice, Taylor & Francis, 2014.

Lectures