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Diffraction methods of analysis

ВКБ.6.04

Вибіркова дисципліна для ОП

First

2022/2023

6 Semester

4

To know principles and procedures of physical, chemical and physico-chemical methods of characterization, typical equipment and devices. Ability to use aquired knowladge and experince for calculations, representation and modelling of chemical systems and processes, treatment of experimental data. To use their knowladhe, understanding, competences and basic engennering and technological skills in practice to solve task and problems of a known nature. To interpret experimental data and find thir correlations with corresponding theories in chemistry.

Full-time form

This course is using knowledge aquired upon studying crystallochemistry (structure and symetry of crystals, point and space elements of symmetry), quantum chemistry (model of atoms, condition of electron transfer between electronic levels in an atom), physics (principles of electromagnetic radiation generation, wave properties of particles, hypotisis of De Broglie, diffraction of waves), mathematics (elements of analytical geometry and vector algebra).

The course "Diffraction Methods of Analysis" is designed to give students an idea of ​​the nature and methods of generating X-rays, the physical basis of continuous and characteristic spectra, the interaction of X-rays with materials, the basic principles of X-ray scattering and its application in structural research. To acquire the material laboratory works are planned, which allow to master the method of processing and interpretation of diffraction images, determining the structural parameters of the unknown substance from the data of X-ray diffraction.

1. Kazimirov V.P., Rusanov E.B. Renthenohrafiia krystalichnykh materialiv: navch. posibnyk – K.: VPTs “Kyivskyi universytet”. – 2016. – 287 s. 2. Kazimirov V.P., Kachur O.V. Renthenohrafiia polikrystaliv: navch. posibnyk – K.: VPTs “Kyivskyi universytet”.– 1994. 3. Cullity B.D., Stock S.R. Elements of X-Ray Diffraction. – Pearson. – 2017. – 654 p. 4. Zolotoyabko E. Basic Concepts of X-Ray Diffraction. – Wiley-VCH. – 2014. – 311 p. 5. Lee M. X-ray diffraction for materials research. From Fundamentals to Applications. – Apple Academic Press. – 2016. – 297 p. 6. P. I. Loboda, O. P. Karasevska, I. Yu. Trosnikova X-ray structural analysis of materials in a dispersed state: academic. manual - Kyiv: Center for Educational Literature, 2017. - 139 p.

Lectures, Laboratory works

Maximum / minimum number of points that can be obtained by a student: 60 points / 36 points, namely: 1. Test №1: 15/8 points. 1. Test №2: 15/8 points. 2. Laboratory works № 1–5: 25/15 points. 4. Evaluation of independent work: 5/3 points. Final assessment (in the form of an exam): Maximum / minimum number of points that can be obtained by a student: 40 points / 24 points.

Ukrainian language