Infopaket

X-Ray Based Research Methods

ВКБ.4.02

Вибіркова дисципліна для ОП

First

2022/2023

5 Semester

3

Р01. Knowledge to understand key chemical concepts, essential facts, concepts, principles, and theories relating to natural sciences, life and earth sciences, as well as chemical technologies at a level sufficient for professional application and to enable further deep understanding of specialized fields of chemistry. Р02. Knowledge to understand the basics of mathematics at a level sufficient to achieve other learning outcomes provided by this guideline and educational program. Р04. Knowledge to understand basic patterns and types of chemical reactions as well as their characteristics. Р05. Knowledge to understand the relationship between structure and properties of substances. Р19. Skill to use your knowledge, understanding, competencies, and basic engineering skills to solve practical tasks and problems of nature. Р21. Ability to monitor and analyze scientific sources of information and professional literature.

Full-time form

Good knowledge of Crystal Chemistry and knowledge of certain sections of Physics, Higher Mathematics and Instrumental Methods of Analysis courses.

X-ray based research methods play a significant role in the crystal structure determination, these methods are also used for determination of the phase composition of crystalline samples and elemental composition. The program of the course "X-Ray Based Research Methods " includes: methods of polychromatic and monochromatic X-rays generation, interaction of X-rays with matter, the conditions for obtaining a diffraction pattern from polycrystalline and monocrystalline samples and X-ray fluorescence spectra. Particular attention is paid to the study of the basics of methods of qualitative and quantitative X-ray phase analysis and X-ray fluorescence analysis.

1. Kazimirov V.P., Rusanov E.B. Radiography of crystalline materials - K.: Kyiv University, 2016. 2. Danylchenko, S.M. X-ray diffraction methods for the study of crystalline materials [Electronic resource]: ed. manual / S.M. Danylchenko, V.M. Kuznetsov, I.Yu. 3. Protsenko. - Electronic version. café Electronics, general and applied physics. - Sumy: Sumy State University, 2019. 4. Pecharesky V., Zavalij P. Fundamentals of Powder Diffraction and Structural Characterization of Materials. - Springer, 2005. 5. V.I. Karmanov, M.S. Slobodianyk, A.O. Kapshuk, S.A. Nedilko. X-ray methods in inorganic chemistry. - K.:, Phytosocial Center, 2001.

Lectures (with the use of computer presentations), laboratory work, self-study

Semester control includes modular tests (written), homework, oral presentations, presentations and defense of laboratory work. The evaluation is based on a 100-point system. Maximum / minimum number of points that can be obtained by a student for a semester grade of 60 points / 36 points. The final assessment is conducted in the form of a written exam. The maximum / minimum number of points that can be obtained by a student in the exam is 40 points / 24 points.

Ukrainian